EAS p-Nitroacetanilide Essay

Pinacol was reborn to pinacolone in the audition at a 15.60% yield. A poor sh are yield was judge callable to the observational distillate and data-based time interval of the two works. some(prenominal) pinacolone could have been trap in the sedimentary layer payable to experimental hallucination at separating via a pipet. The IR showed peaks at 2967, 2906, 2871, 2359, 2337, 2173, and 1989. The re kick inative peaks in an IR of pinacolene are present amidst 3000 and 1700. The proton magnetic resonance when manipulated with a six-fold of three, showed the presence of 9 hydrogens at 1.2 ppm and 3 hydrogens at 2.1 ppm. The true proton magnetic resonance for pinacolone shows peaks around 20, 40, and 70 ppm due to the negativity of the type O present in the compound. The nuclear magnetic resonance of the essential harvest-tide is inconsistent with the typical NMR of pinacolone or water. This could potentially be due to a mixture of the two compounds when the NMR w as run and is due to the experimental error in the separation of the aqueous and organic layers by pipet. Pinacol was converted to pinacolone in the experiment at a 15.60% yield.A low percent yield was expected due to the experimental distillation and experimental separation of the two layers. Some pinacolone could have been trapped in the aqueous layer due to experimental error at separating via a pipet. The IR showed peaks at 2967, 2906, 2871, 2359, 2337, 2173, and 1989. The representative peaks in an IR of pinacolene are present between 3000 and 1700. The NMR when manipulated with a multiple of three, showed the presence of 9 hydrogens at 1.2 ppm and 3 hydrogens at 2.1 ppm. The typical NMR for pinacolone shows peaks around 20, 40, and 70 ppm due to the electronegativity of the oxygen present in the compound. The NMR of the organic product is inconsistent with the typical NMR of pinacolone or water. This could potentially be due to a mixture of the two compounds when the NMR was r un and is due to the experimental error in the separation of the aqueous and organic layers by pipet.Pinacol was converted to pinacolone in the experiment at a 15.60% yield. A low percent yield was expected due to the experimental distillation and experimental separation of the two layers. Some pinacolone could have been trapped in the aqueous layer due to experimental error at separating via a pipet. The IR showed peaks at 2967, 2906, 2871, 2359, 2337, 2173, and 1989. The representative peaks in an IR of pinacolene are present between 3000 and 1700. The NMR when manipulated with a multiple of three, showed the presence of 9 hydrogens at 1.2 ppm and 3 hydrogens at 2.1 ppm. The typical NMR forpinacolone shows peaks around 20, 40, and 70 ppm due to the electronegativity of the oxygen present in the compound. The NMR of the organic product is inconsistent with the typical NMR of pinacolone or water. This could potentially be due to a mixture of the two compounds when the NMR was run an d is due to the experimental error in the separation of the aqueous and organic layers by pipet.Pinacol was converted to pinacolone in the experiment at a 15.60% yield. A low percent yield was expected due to the experimental distillation and experimental separation of the two layers.Some pinacolone could have been trapped in the aqueous layer due to experimental error at separating via a pipet. The IR showed peaks at 2967, 2906, 2871, 2359, 2337, 2173, and 1989. The representative peaks in an IR of pinacolene are present between 3000 and 1700. The NMR when manipulated with a multiple of three, showed the presence of 9 hydrogens at 1.2 ppm and 3 hydrogens at 2.1 ppm. The typical NMR for pinacolone shows peaks around 20, 40, and 70 ppm due to the electronegativity of the oxygen present in the compound. The NMR of the organic product is inconsistent with the typical NMR of pinacolone or water. This could potentially be due to a mixture of the two compounds when the NMR was run and is due to the experimental error in the separation of the aqueous and organic layers by pipet.Pinacol was converted to pinacolone in the experiment at a 15.60% yield. A low percent yield was expected due to the experimental distillation and experimental separation of the two layers. Some pinacolone could have been trapped in the aqueous layer due to experimental error at separating via a pipet. The IR showed peaks at 2967, 2906, 2871, 2359, 2337, 2173, and 1989. The representative peaks in an IR of pinacolene are present between 3000 and 1700. The NMR when manipulated with a multiple of three, showed the presence of 9 hydrogens at 1.2 ppm and 3 hydrogens at 2.1 ppm. The typical NMR for pinacolone shows peaks around 20, 40, and 70 ppm due to the electronegativity of the oxygen present in the compound. The NMR of the organic product is inconsistent with the typical NMR of pinacolone or water. This could potentially be due to a mixture of the two compounds when the NMR was run and is due to the experimental error in the separation of the aqueous and organic layers by pipet.